TA Instruments

AR1756-0005f

15/03/2013 14:50:28

Sample name	ASW Blank coupon#20 + DI + beads 250rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	5 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:50:28

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 250.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	249.9	-360.15	10000	20.0	0.1461	0.996	-117.4	312.4	-0.3758	595.2	204.0430	6.099E-3	255.05	25505	3.411E-3	0.0	0.0
1.9960	250.0	488.18	10000	20.0	0.1323	1.996	159.1	312.5	0.5093	539.0	404.0640	5.521E-3	505.08	50508	3.411E-3	0.0	0.0
2.9960	250.0	488.11	10000	20.0	0.1299	2.996	159.1	312.5	0.5091	529.1	707.2210	5.418E-3	884.03	88403	3.411E-3	0.0	0.0
3.9960	250.0	491.09	10000	20.0	0.1268	3.996	160.1	312.5	0.5122	516.7	906.5910	5.291E-3	1133.2	1.1332E5	3.411E-3	0.1	0.1
4.9960	250.0	483.93	10000	20.0	0.1234	4.996	157.7	312.5	0.5048	502.6	1208.4100	5.147E-3	1510.5	1.5105E5	3.411E-3	0.1	0.1
5.9920	250.0	489.24	10000	20.0	0.1254	5.992	159.5	312.5	0.5103	510.9	1409.0601	5.231E-3	1761.3	1.7613E5	3.411E-3	0.1	0.1
6.9920	250.0	485.69	10000	20.0	0.1240	6.992	158.3	312.5	0.5066	505.1	1710.7100	5.173E-3	2138.4	2.1384E5	3.411E-3	0.1	0.1
7.9920	250.0	481.95	10000	20.0	0.1260	7.992	157.1	312.5	0.5027	513.3	1916.7900	5.256E-3	2396.0	2.3960E5	3.411E-3	0.1	0.1
8.9880	250.0	468.94	10000	20.0	0.1292	8.988	152.9	312.5	0.4891	526.6	2213.5500	5.391E-3	2766.9	2.7669E5	3.411E-3	0.1	0.1
9.9920	250.0	468.05	10000	20.0	0.1238	9.992	152.6	312.5	0.4882	504.3	2417.3899	5.163E-3	3021.7	3.0217E5	3.411E-3	0.2	0.2
10.992	250.0	468.89	10000	20.0	0.1270	10.992	152.8	312.5	0.4891	517.5	2715.9700	5.299E-3	3395.0	3.3950E5	3.411E-3	0.2	0.2
11.992	250.0	480.33	10000	20.0	0.1250	11.992	156.6	312.5	0.5010	509.2	2917.0400	5.213E-3	3646.3	3.6463E5	3.411E-3	0.2	0.2
12.992	250.0	476.54	10000	20.0	0.1315	12.992	155.3	312.5	0.4971	535.7	3218.7100	5.486E-3	4023.4	4.0234E5	3.411E-3	0.2	0.2
13.992	250.0	480.50	10000	20.0	0.1262	13.992	156.6	312.5	0.5012	514.2	3419.6001	5.265E-3	4274.5	4.2745E5	3.411E-3	0.2	0.2
14.992	250.0	483.82	10000	20.0	0.1240	14.992	157.7	312.5	0.5047	505.1	3721.3101	5.172E-3	4651.6	4.6516E5	3.411E-3	0.2	0.2
15.992	250.0	476.91	10000	20.0	0.1205	15.992	155.4	312.5	0.4974	491.0	3923.4299	5.028E-3	4904.3	4.9043E5	3.411E-3	0.3	0.3
16.992	250.0	481.75	10000	20.0	0.1288	16.992	157.0	312.5	0.5025	524.9	4224.7002	5.376E-3	5280.9	5.2809E5	3.411E-3	0.3	0.3
17.992	250.0	476.81	10000	20.0	0.1244	17.992	155.4	312.5	0.4973	506.7	4424.9102	5.189E-3	5531.1	5.5311E5	3.411E-3	0.3	0.3
18.996	250.0	479.95	10000	20.0	0.1238	18.996	156.4	312.5	0.5006	504.3	4727.6699	5.163E-3	5909.6	5.9096E5	3.411E-3	0.3	0.3
19.992	250.0	473.29	10000	20.0	0.1303	19.992	154.3	312.5	0.4937	530.7	4927.5400	5.435E-3	6159.4	6.1594E5	3.411E-3	0.3	0.3
20.992	250.0	473.49	10000	20.0	0.1238	20.992	154.3	312.5	0.4939	504.3	5229.2700	5.164E-3	6536.6	6.5366E5	3.411E-3	0.3	0.3
21.992	250.0	469.85	10000	20.0	0.1248	21.992	153.1	312.5	0.4901	508.4	5431.3599	5.206E-3	6789.2	6.7892E5	3.411E-3	0.4	0.4
22.992	250.0	495.01	10000	20.0	0.1215	22.992	161.3	312.5	0.5163	495.2	5731.7500	5.071E-3	7164.7	7.1647E5	3.411E-3	0.4	0.4
23.992	250.0	476.10	10000	20.0	0.1213	23.992	155.2	312.5	0.4966	494.3	5934.7100	5.061E-3	7418.4	7.4184E5	3.411E-3	0.4	0.4
24.996	250.0	484.89	10000	20.0	0.1209	24.996	158.1	312.5	0.5057	492.7	6234.4902	5.045E-3	7793.1	7.7931E5	3.411E-3	0.4	0.4
25.992	250.0	488.81	10000	20.0	0.1225	25.992	159.3	312.5	0.5098	499.3	6436.8999	5.112E-3	8046.1	8.0461E5	3.411E-3	0.4	0.4
26.992	250.0	481.91	10000	20.0	0.1219	26.992	157.1	312.5	0.5027	496.8	6737.1499	5.088E-3	8421.4	8.4214E5	3.411E-3	0.4	0.4
27.992	250.0	472.68	10000	20.0	0.1258	27.992	154.1	312.5	0.4930	512.5	6942.5200	5.248E-3	8678.2	8.6782E5	3.411E-3	0.5	0.5
28.996	250.0	474.48	10000	20.0	0.1248	28.996	154.7	312.5	0.4949	508.4	7239.7998	5.206E-3	9049.8	9.0498E5	3.411E-3	0.5	0.5
29.992	250.0	482.82	10000	20.0	0.1242	29.992	157.4	312.5	0.5036	505.9	7442.5898	5.180E-3	9303.2	9.3032E5	3.411E-3	0.5	0.5
30.992	250.0	479.95	10000	20.0	0.1185	30.992	156.4	312.5	0.5006	482.8	7745.6802	4.943E-3	9682.1	9.6821E5	3.411E-3	0.5	0.5
31.996	250.0	482.69	10000	20.0	0.1238	31.996	157.3	312.5	0.5035	504.3	7943.3799	5.165E-3	9929.2	9.9292E5	3.411E-3	0.5	0.5
32.992	250.0	477.68	10000	20.0	0.1236	32.992	155.7	312.5	0.4982	503.4	8249.4004	5.155E-3	10312	1.0312E6	3.411E-3	0.5	0.5
33.996	250.0	476.42	10000	20.0	0.1250	33.996	155.3	312.5	0.4970	509.2	8447.4805	5.215E-3	10559	1.0559E6	3.411E-3	0.6	0.6
34.992	250.0	482.10	10000	20.0	0.1250	34.992	157.1	312.6	0.5028	509.2	8750.0898	5.213E-3	10938	1.0938E6	3.411E-3	0.6	0.6
35.992	250.0	487.19	10000	20.0	0.1213	35.992	158.8	312.5	0.5082	494.3	8948.8896	5.062E-3	11186	1.1186E6	3.411E-3	0.6	0.6
36.988	250.0	478.10	10000	20.0	0.1232	36.988	155.8	312.5	0.4987	501.8	9252.4102	5.138E-3	11566	1.1566E6	3.411E-3	0.6	0.6
37.992	250.0	479.70	10000	20.0	0.1248	37.992	156.4	312.5	0.5003	508.4	9452.0898	5.206E-3	11815	1.1815E6	3.411E-3	0.6	0.6
38.996	250.0	482.58	10000	20.0	0.1215	38.996	157.3	312.5	0.5034	495.2	9753.9004	5.071E-3	12192	1.2192E6	3.411E-3	0.6	0.6
39.992	250.0	474.89	10000	20.0	0.1187	39.992	154.8	312.5	0.4953	483.6	9954.0303	4.952E-3	12443	1.2443E6	3.411E-3	0.7	0.7
40.992	250.0	478.16	10000	20.0	0.1244	40.992	155.9	312.5	0.4988	506.7	10155.000	5.189E-3	12694	1.2694E6	3.411E-3	0.7	0.7
41.992	250.0	481.51	10000	20.0	0.1282	41.992	156.9	312.5	0.5022	522.4	10456.700	5.350E-3	13071	1.3071E6	3.411E-3	0.7	0.7
42.996	250.0	477.93	10000	20.0	0.1270	42.996	155.8	312.5	0.4985	517.5	10657.700	5.298E-3	13322	1.3322E6	3.411E-3	0.7	0.7
43.992	250.0	479.78	10000	20.0	0.1165	43.992	156.4	312.5	0.5004	474.5	10959.500	4.859E-3	13699	1.3699E6	3.411E-3	0.7	0.7
44.992	250.0	483.00	10000	20.0	0.1270	44.992	157.4	312.5	0.5038	517.5	11161.400	5.300E-3	13952	1.3952E6	3.411E-3	0.7	0.7
45.992	250.0	475.60	10000	20.0	0.1242	45.992	155.0	312.5	0.4960	505.9	11462.000	5.180E-3	14328	1.4328E6	3.411E-3	0.8	0.8
47.000	250.0	485.72	10000	20.0	0.1286	47.000	158.3	312.5	0.5066	524.1	11663.100	5.367E-3	14579	1.4579E6	3.411E-3	0.8	0.8
47.992	250.0	485.10	10000	20.0	0.1225	47.992	158.1	312.5	0.5060	499.3	11972.500	5.113E-3	14966	1.4966E6	3.411E-3	0.8	0.8
48.992	250.0	476.20	10000	20.0	0.1294	48.992	155.2	312.5	0.4967	527.4	12165.700	5.400E-3	15207	1.5207E6	3.411E-3	0.8	0.8
49.988	250.0	481.18	10000	20.0	0.1264	49.988	156.8	312.5	0.5019	515.0	12467.100	5.274E-3	15584	1.5584E6	3.411E-3	0.8	0.8
50.988	250.0	470.63	10000	20.0	0.1264	50.988	153.4	312.5	0.4909	515.0	12668.300	5.273E-3	15835	1.5835E6	3.411E-3	0.8	0.8
51.992	250.0	481.64	10000	20.0	0.1266	51.992	157.0	312.5	0.5023	515.8	12969.800	5.281E-3	16212	1.6212E6	3.411E-3	0.9	0.9
52.992	250.0	476.35	10000	20.0	0.1284	52.992	155.3	312.5	0.4968	523.3	13173.000	5.358E-3	16466	1.6466E6	3.411E-3	0.9	0.9
53.992	250.0	475.17	10000	20.0	0.1282	53.992	154.9	312.5	0.4956	522.4	13472.600	5.350E-3	16841	1.6841E6	3.411E-3	0.9	0.9
54.992	250.0	475.08	10000	20.0	0.1205	54.992	154.9	312.5	0.4955	491.0	13673.600	5.028E-3	17092	1.7092E6	3.411E-3	0.9	0.9
55.992	250.0	479.72	10000	20.0	0.1246	55.992	156.4	312.5	0.5004	507.6	13975.100	5.198E-3	17469	1.7469E6	3.411E-3	0.9	0.9
56.996	250.0	485.91	10000	20.0	0.1203	56.996	158.4	312.5	0.5069	490.2	14177.300	5.021E-3	17722	1.7722E6	3.411E-3	0.9	0.9
57.992	250.0	484.32	10000	20.0	0.1250	57.992	157.9	312.5	0.5052	509.2	14479.500	5.215E-3	18099	1.8099E6	3.411E-3	1.0	1.0
58.996	250.0	480.54	10000	20.0	0.1254	58.996	156.6	312.5	0.5012	510.9	14682.500	5.232E-3	18353	1.8353E6	3.411E-3	1.0	1.0
59.996	250.0	485.92	10000	20.0	0.1266	59.996	158.4	312.5	0.5068	515.8	14980.400	5.282E-3	18726	1.8726E6	3.411E-3	1.0	1.0

